MARC details
000 -LEADER |
fixed length control field |
08667nam a2200541 a 4500 |
001 - CONTROL NUMBER |
control field |
BDZ0006629490 |
003 - CONTROL NUMBER IDENTIFIER |
control field |
StDuBDS |
005 - DATE AND TIME OF LATEST TRANSACTION |
control field |
20180923143644.0 |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
fixed length control field |
041210s2005 stka f b 001|0|eng d |
010 ## - LIBRARY OF CONGRESS CONTROL NUMBER |
LC control number |
2004062930 |
020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
International Standard Book Number |
9780443074455 (pbk.) : |
Terms of availability |
�29.99 |
020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
International Standard Book Number |
0443074453 |
Terms of availability |
�37.49 |
035 ## - SYSTEM CONTROL NUMBER |
System control number |
(DNLM)101236760 |
040 ## - CATALOGING SOURCE |
Original cataloging agency |
StDuBDS |
Language of cataloging |
eng |
Transcribing agency |
StDuBDS |
Modifying agency |
StDuBDSZ |
042 ## - AUTHENTICATION CODE |
Authentication code |
pcc |
050 #4 - LIBRARY OF CONGRESS CALL NUMBER |
Classification number |
RS403 |
072 #7 - SUBJECT CATEGORY CODE |
Subject category code |
HEA |
Source |
ukslc |
072 #7 - SUBJECT CATEGORY CODE |
Subject category code |
MKG |
Source |
thema |
082 0# - DEWEY DECIMAL CLASSIFICATION NUMBER |
Classification number |
615.1901 WAT |
100 1# - MAIN ENTRY--PERSONAL NAME |
Personal name |
Watson, David G., |
Dates associated with a name |
1952- |
245 10 - TITLE STATEMENT |
Title |
Pharmaceutical analysis : |
Remainder of title |
a textbook for pharmacy students and pharmaceutical chemists / |
Statement of responsibility, etc. |
David G. Watson. |
250 ## - EDITION STATEMENT |
Edition statement |
2nd ed. |
260 ## - PUBLICATION, DISTRIBUTION, ETC. |
Place of publication, distribution, etc. |
Edinburgh : |
Name of publisher, distributor, etc. |
Elsevier Churchill Livingstone, |
Date of publication, distribution, etc. |
2005. |
300 ## - PHYSICAL DESCRIPTION |
Extent |
xiii, 382 p. : |
Other physical details |
ill. ; |
Dimensions |
25 cm. |
500 ## - GENERAL NOTE |
General note |
Previous ed.: 1999. |
504 ## - BIBLIOGRAPHY, ETC. NOTE |
Bibliography, etc. note |
Includes bibliographical references and index. |
505 0# - FORMATTED CONTENTS NOTE |
Formatted contents note |
1.Control of the quality of analytical methods:- Introduction--Control of errors in analysis--Accuracy and precision--Validation of analytical procedures--Standard operating procedure (SOP) for the assay of paracetamol tablets--Compound random errors--Reporting of results--Other terms used in the control analytical procedures--Basic calculations in pharmaceutical analysis--Additional problems -- 2.Physical and chemical properties of drug molecules:- Introduction--Calculation of pH value of aqueous solutions of strong and weak acids and bases--Acidic and basic strength and pKa--Henderson-Hasselbalch equation--Ionisation of drug molecules--Buffers--Salt hydrolysis--Activity, ionic strength and dielectric constant--Partition coefficient--Drug stability--Stereochemistry of drugs--Measurement of optical rotation--Profiles of physico-chemical properties of some drug molecules--Additional problems--3. Titrimetric and chemical analysis methods:- Keypoints--Introduction--Instrumentation and reagents--Direct acid/base titrations in the aqueous phase--Titration of the salts of weak bases in mixed aqueous/non-aqueous media--Indirect titrations in the aqueous phase--Non-aqueous titrations--Argentimetric titrations--Compleximetric titrations--Redox titrations--Iodometric titrations--Ion pair titrations--Diazotisation titrations--Potentiometric titrations--Karl Fischer titration (coulometric end-point detection)--Automation of wet chemical methods--Applications of FIA in pharmaceutical analysis--Additional problems--4. Ultraviolet and visible spectroscopy:- Keypoints--Introduction--Factors governing absorption of radiation in the UV/visible region--Beer-Lambert Law--Instrumentation--Diode array instruments--Instrument calibration--UV spectra of some representative drug modules--Use of UV/visible spectrophotometry to determine pKa values--~Applications of UV/visible spectrophotometry to pharmaceutical quantitative analysis--Difference spectrophotometry-- Derrivative spectra--Applications of UV/visible spectrophotometry in preformulation and formulation--Additional problems -- 5. Infrared spectrophotometry :- Keypoints--Introduction--Factors determining intensity and energy level of absorption in IR spectra--Instrumentation--Sample preparation--Application of IR spectrophotometry in structure elucidation--Example of IR spectra of drug molecules--IR spectrophotometry as a fingerprint technique--Infrared spectrophotometry as a method for identifying polymorphs--Near-infrared analysis(NIRA)--Key points--Introduction--Examples of NIRA application--Additional problems-- 6.Atomic spectrophotometry:- Atomic emission spectrophotometry: Keypoints--Introduction--Instrumentation--Examples of quantitation by AES--Interferences in AES analysis--Assays based on the method of standard additions--Atomic Absorption spectrophotometry: Keypoints--Introduction--Instrumentation--Examples of assays using AAS--Some examples of limit tests employing AAS-Inductivity coupled plasma emission spectrophotometry -- 7. Molecular emission spectroscopy:- Fluorescence spectroscopy--Keypoints--Introduction--Instrumentation--Molecules which exhibit fluorescence--Factors interfering with fluorescence intensity--Applications of fluorescence spectrophotometry in pharmaceutical analysis--Raman spectroscopy: Keypoints--Introduction--Instrumentation--Applications -- 8.Nuclear magnetic resonance spectroscopy:- Keypoints--Introduction--Instrumentation--Proton NMR--Application of NMR to structure onfirmation in some drug molecules--Carbon-13 NMR--Two dimensional NMR spectra--Application of NMR to quantitive analysis--Other specialised applications of NMR -- 9.Mass spectrometry:- Keypoints--Introduction--Instrumentation--Mass spectra obtained under election impact (EI) ionisation conditions--Molecular fragmentation patterns--EI mass spectra of some drug molecules--Gas chromatography- mass spectrometry (GC - MS)--Applications of GC-MS to impurity profiling--Liquid chromatography- mass spectrometry (LC-MS)--Some examples of tandem mass spectra--Applications of LC-MS in pharmaceutical analysis -- 10.Chromatographic theory:- Introduction--Void volume and capacity factor--Calculation of column efficiency--Origins of band broadening in HPLC--Parameters used in evaluating column performance--Data acquisition--Report generation -- 11.Gas chromatography :- Keypoints--Introduction--Instrumentation--Selectivity of liquid stationary phases--Use of derivatisation in GC--Summary of paramaters governing capillary GC performance--GC detectors-- Applications of GCin quantitative analysis--Determination of manufacturing and degradation residues by GC--Determination of residual solvents--Solid-phase microextraction (SPME)--Applications of GC in bioanalysis--Additional problems-- 12.High-pressure liquid chromatography:- Keypoints--Introduction--Instrumentation--Stationary and mobile phases--Structural factors which govern rate of elution of compounds from HPLC columns--More advanced consieration of solvent selectivity in reverse-phase chromatography--Summary of stationary phases used in HPLC--A more advanced consideration of reverse-phase stationery phases--Summary of detectors used in HPLC--Performance of a diode array detector (DAD)-- Applications of HPLC to the quantitative analysis of drugs in formulations--Assays involving more specialised HPLC techniques--Additional problems -- 13.Thin layer chromatography :- Keypoints--Introduction--Instrumentation--TLC chromatogram--Stationary phases-- Elutropic series and mobile phases--Modification of TLC adsorbant--Detection of compounds on TLC plates following development--Applications of TLC analysis--High-performance TLC (HPTLC)-- 14.High-performance capillary electrophoresis:- Keypoints--Introduction--Instrumentation--Control of separation--Applications of CE in pharmaceutical analysis--Additional problems -- 15.Extraction methods in pharmaceutical analysis:- Keypoints--Introduction--Commonly used excipients in formulations--Solvent extraction methods--Solid-phase extraction (SPE)--Keypoints--Introduction--Methodology--Types of adsorbants used in SPE--Adaptation of SPE for automated on-ine extraction prior to HPLC analysis--Recent developments in solid-phase and on-line extraction. |
520 8# - SUMMARY, ETC. |
Summary, etc. |
'Pharmaceutical Analysis' is aimed primarily at pharmacy students and pharmaceutical chemists. It highlights the most important aspects of a wide range of techniques used in the control of the quality of pharmaceuticals. |
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Drugs |
General subdivision |
Analysis |
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Pharmaceutical chemistry. |
650 #7 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Pharmacology |
Source of heading or term |
thema |
650 #7 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Health and Wellbeing. |
Source of heading or term |
ukslc |
650 12 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Pharmaceutical Preparations |
General subdivision |
analysis |
650 22 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Chromatography |
General subdivision |
methods |
650 22 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Spectrophotometry |
General subdivision |
methods |
650 22 - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Spectrum Analysis |
General subdivision |
methods |
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961 ## - REQUESTOR & SELECTOR |
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stg30.74 |
Selector |
Grainne O'Malley |
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main |
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Jo Corkery |
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Internal note |
claim1 was sent 04-10-2010 |
Selector |
Michael - Pharmacy Technician Books |
-- |
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m |
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