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Pharmaceutical analysis : (Record no. 8778)

MARC details
000 -LEADER
fixed length control field 08667nam a2200541 a 4500
001 - CONTROL NUMBER
control field BDZ0006629490
003 - CONTROL NUMBER IDENTIFIER
control field StDuBDS
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20180923143644.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 041210s2005 stka f b 001|0|eng d
010 ## - LIBRARY OF CONGRESS CONTROL NUMBER
LC control number 2004062930
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number 9780443074455 (pbk.) :
Terms of availability �29.99
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number 0443074453
Terms of availability �37.49
035 ## - SYSTEM CONTROL NUMBER
System control number (DNLM)101236760
040 ## - CATALOGING SOURCE
Original cataloging agency StDuBDS
Language of cataloging eng
Transcribing agency StDuBDS
Modifying agency StDuBDSZ
042 ## - AUTHENTICATION CODE
Authentication code pcc
050 #4 - LIBRARY OF CONGRESS CALL NUMBER
Classification number RS403
072 #7 - SUBJECT CATEGORY CODE
Subject category code HEA
Source ukslc
072 #7 - SUBJECT CATEGORY CODE
Subject category code MKG
Source thema
082 0# - DEWEY DECIMAL CLASSIFICATION NUMBER
Classification number 615.1901 WAT
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Watson, David G.,
Dates associated with a name 1952-
245 10 - TITLE STATEMENT
Title Pharmaceutical analysis :
Remainder of title a textbook for pharmacy students and pharmaceutical chemists /
Statement of responsibility, etc. David G. Watson.
250 ## - EDITION STATEMENT
Edition statement 2nd ed.
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Edinburgh :
Name of publisher, distributor, etc. Elsevier Churchill Livingstone,
Date of publication, distribution, etc. 2005.
300 ## - PHYSICAL DESCRIPTION
Extent xiii, 382 p. :
Other physical details ill. ;
Dimensions 25 cm.
500 ## - GENERAL NOTE
General note Previous ed.: 1999.
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references and index.
505 0# - FORMATTED CONTENTS NOTE
Formatted contents note 1.Control of the quality of analytical methods:- Introduction--Control of errors in analysis--Accuracy and precision--Validation of analytical procedures--Standard operating procedure (SOP) for the assay of paracetamol tablets--Compound random errors--Reporting of results--Other terms used in the control analytical procedures--Basic calculations in pharmaceutical analysis--Additional problems -- 2.Physical and chemical properties of drug molecules:- Introduction--Calculation of pH value of aqueous solutions of strong and weak acids and bases--Acidic and basic strength and pKa--Henderson-Hasselbalch equation--Ionisation of drug molecules--Buffers--Salt hydrolysis--Activity, ionic strength and dielectric constant--Partition coefficient--Drug stability--Stereochemistry of drugs--Measurement of optical rotation--Profiles of physico-chemical properties of some drug molecules--Additional problems--3. Titrimetric and chemical analysis methods:- Keypoints--Introduction--Instrumentation and reagents--Direct acid/base titrations in the aqueous phase--Titration of the salts of weak bases in mixed aqueous/non-aqueous media--Indirect titrations in the aqueous phase--Non-aqueous titrations--Argentimetric titrations--Compleximetric titrations--Redox titrations--Iodometric titrations--Ion pair titrations--Diazotisation titrations--Potentiometric titrations--Karl Fischer titration (coulometric end-point detection)--Automation of wet chemical methods--Applications of FIA in pharmaceutical analysis--Additional problems--4. Ultraviolet and visible spectroscopy:- Keypoints--Introduction--Factors governing absorption of radiation in the UV/visible region--Beer-Lambert Law--Instrumentation--Diode array instruments--Instrument calibration--UV spectra of some representative drug modules--Use of UV/visible spectrophotometry to determine pKa values--~Applications of UV/visible spectrophotometry to pharmaceutical quantitative analysis--Difference spectrophotometry-- Derrivative spectra--Applications of UV/visible spectrophotometry in preformulation and formulation--Additional problems -- 5. Infrared spectrophotometry :- Keypoints--Introduction--Factors determining intensity and energy level of absorption in IR spectra--Instrumentation--Sample preparation--Application of IR spectrophotometry in structure elucidation--Example of IR spectra of drug molecules--IR spectrophotometry as a fingerprint technique--Infrared spectrophotometry as a method for identifying polymorphs--Near-infrared analysis(NIRA)--Key points--Introduction--Examples of NIRA application--Additional problems-- 6.Atomic spectrophotometry:- Atomic emission spectrophotometry: Keypoints--Introduction--Instrumentation--Examples of quantitation by AES--Interferences in AES analysis--Assays based on the method of standard additions--Atomic Absorption spectrophotometry: Keypoints--Introduction--Instrumentation--Examples of assays using AAS--Some examples of limit tests employing AAS-Inductivity coupled plasma emission spectrophotometry -- 7. Molecular emission spectroscopy:- Fluorescence spectroscopy--Keypoints--Introduction--Instrumentation--Molecules which exhibit fluorescence--Factors interfering with fluorescence intensity--Applications of fluorescence spectrophotometry in pharmaceutical analysis--Raman spectroscopy: Keypoints--Introduction--Instrumentation--Applications -- 8.Nuclear magnetic resonance spectroscopy:- Keypoints--Introduction--Instrumentation--Proton NMR--Application of NMR to structure onfirmation in some drug molecules--Carbon-13 NMR--Two dimensional NMR spectra--Application of NMR to quantitive analysis--Other specialised applications of NMR -- 9.Mass spectrometry:- Keypoints--Introduction--Instrumentation--Mass spectra obtained under election impact (EI) ionisation conditions--Molecular fragmentation patterns--EI mass spectra of some drug molecules--Gas chromatography- mass spectrometry (GC - MS)--Applications of GC-MS to impurity profiling--Liquid chromatography- mass spectrometry (LC-MS)--Some examples of tandem mass spectra--Applications of LC-MS in pharmaceutical analysis -- 10.Chromatographic theory:- Introduction--Void volume and capacity factor--Calculation of column efficiency--Origins of band broadening in HPLC--Parameters used in evaluating column performance--Data acquisition--Report generation -- 11.Gas chromatography :- Keypoints--Introduction--Instrumentation--Selectivity of liquid stationary phases--Use of derivatisation in GC--Summary of paramaters governing capillary GC performance--GC detectors-- Applications of GCin quantitative analysis--Determination of manufacturing and degradation residues by GC--Determination of residual solvents--Solid-phase microextraction (SPME)--Applications of GC in bioanalysis--Additional problems-- 12.High-pressure liquid chromatography:- Keypoints--Introduction--Instrumentation--Stationary and mobile phases--Structural factors which govern rate of elution of compounds from HPLC columns--More advanced consieration of solvent selectivity in reverse-phase chromatography--Summary of stationary phases used in HPLC--A more advanced consideration of reverse-phase stationery phases--Summary of detectors used in HPLC--Performance of a diode array detector (DAD)-- Applications of HPLC to the quantitative analysis of drugs in formulations--Assays involving more specialised HPLC techniques--Additional problems -- 13.Thin layer chromatography :- Keypoints--Introduction--Instrumentation--TLC chromatogram--Stationary phases-- Elutropic series and mobile phases--Modification of TLC adsorbant--Detection of compounds on TLC plates following development--Applications of TLC analysis--High-performance TLC (HPTLC)-- 14.High-performance capillary electrophoresis:- Keypoints--Introduction--Instrumentation--Control of separation--Applications of CE in pharmaceutical analysis--Additional problems -- 15.Extraction methods in pharmaceutical analysis:- Keypoints--Introduction--Commonly used excipients in formulations--Solvent extraction methods--Solid-phase extraction (SPE)--Keypoints--Introduction--Methodology--Types of adsorbants used in SPE--Adaptation of SPE for automated on-ine extraction prior to HPLC analysis--Recent developments in solid-phase and on-line extraction.
520 8# - SUMMARY, ETC.
Summary, etc. 'Pharmaceutical Analysis' is aimed primarily at pharmacy students and pharmaceutical chemists. It highlights the most important aspects of a wide range of techniques used in the control of the quality of pharmaceuticals.
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Drugs
General subdivision Analysis
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Pharmaceutical chemistry.
650 #7 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Pharmacology
Source of heading or term thema
650 #7 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Health and Wellbeing.
Source of heading or term ukslc
650 12 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Pharmaceutical Preparations
General subdivision analysis
650 22 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Chromatography
General subdivision methods
650 22 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Spectrophotometry
General subdivision methods
650 22 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Spectrum Analysis
General subdivision methods
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960 ## - PHYSICAL LOCATION (RLIN)
Physical location, PLOC (RLIN) main
Copies 1
Cataloging date 070307
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Estimated price 45.35
Form – physical form b
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Order date 2005-07-05
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Language eng
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960 ## - PHYSICAL LOCATION (RLIN)
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Code1 -
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Order date 2010-07-21
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961 ## - REQUESTOR & SELECTOR
Foreign currency stg30.74
Selector Grainne O'Malley
Locations main
Funds none
961 ## - REQUESTOR & SELECTOR
Foreign currency stg29.99
Selector Jo Corkery
Locations main
Funds none
961 ## - REQUESTOR & SELECTOR
Foreign currency gbp44.07
Internal note claim1 was sent 04-10-2010
Selector Michael - Pharmacy Technician Books
-- Order printed 21-07-2010 15:14
Locations nlib
Funds none
998 ## - LOCAL CONTROL INFORMATION (RLIN)
Operator's initials, OID (RLIN) 9
Cataloger's initials, CIN (RLIN) 050705
First Date, FD (RLIN) m
Local a
-- -
-- 0
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Home library Current library Shelving location Date acquired Cost, normal purchase price Total Checkouts Total Renewals Full call number Barcode Date last seen Date last checked out Copy number Cost, replacement price Price effective from Koha item type
    Dewey Decimal Classification     TUS: Midlands, Main Library TUS: Midlands, Main Library Athlone Nursing Collection 26/11/2010 37.49 4 8 615.1901 WAT 00214202 09/11/2022 28/10/2022 1 37.49 14/08/2017 Long Loan
    Dewey Decimal Classification     TUS: Midlands, Main Library TUS: Midlands, Main Library Athlone General Lending 09/01/2006 37.49 43 65 615.1901 WAT 128202 22/04/2022 24/03/2022 1 37.49 14/08/2017 Long Loan
    Dewey Decimal Classification     TUS: Midlands, Main Library TUS: Midlands, Main Library Athlone General Lending 12/08/2005 31.00 60 59 615.1901 WAT 00211376 25/10/2022 15/09/2022 1 31.00 14/08/2017 Short Loan

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