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Analytical chemistry / D. Kealey and P.J. Haines.

By: Contributor(s): Material type: TextTextSeries: Instant notes | Instant notesPublication details: Oxford : BIOS Scientific, 2002.Description: x, 342 p. : ill. ; 25 cmISBN:
  • 9781859961896 (pbk.) :
  • 1859961894(pbk.)
Subject(s): DDC classification:
  • 543 KEA
Contents:
Section A NATURE AND SCOPE OF ANALYTICAL CHEMISTRY. Analytical chemistry, its functions and applications. Analytical problems and procedures. Analytical techniques and methods. Sampling and sample handling. Calibration and standards. Quality in analytical laboratories. Section B ASSESMENT OF DATA. Errors in analytical measurements. Assessment of accuracy and precision. Significance testing. Calibration and linear regression. Quality control and chemometrics. Section C ANALYTICAL REACTIONS IN SOLUTION. Solution equilibria. Electrochemical reactions. Potentiometry. pH and its control. Titrimetry I: acid-base titrations. Complexation, solubility and redox equilibria. Titrimetry II: complexation, precipitation and redox titrations. Gravimetry. Voltammetry and amperometry. Conductimetry. Section D SEPARATION TECHNIQUES. Solvent and solid phase extraction. Principles of chromatography. Thin-layer chromatography. Gas chromatography: principles and instrumentation. Gas chromatography: procedures and applications. High-performance liquid chromatography: principles and instrumentation. High performance liquid chromatography: modes, procedures and applications. Electrophoresis and electrochromatography: principles and instrumentation. Electrophoresis and electrochromatography: modes, procedures and applications. Section E SPECTROMETRIC TECHNIQUES. Electromagnetic radiation and energy levels. Atomic and molecular spectrometry. Spectrometric instrumentation. Flame atomic emission spectrometry. Inductively coupled plasma spectrometry. X-ray emission spectrometry. Atomic absorbance and fluorescence spectrometry. Ultraviolet and visible molecular spectrometry: principles and instrumentation. Ultraviolet and visible molecular spectrometry: applications. Infrared and raman spectrometry: principles and instrumentation. Infrared and raman spectrometry: sample preparation and spectral interpretation. Nuclear magnetic resonance spectrometry: principles and instrumentation. Nuclear magnetic resonance spectrometry: interpretation of proton and carbon-13 spectra. Mass spectrometry. Section F COMBINED TECHNIQUES. Advantages of combined techniques. Sample identification using multiple spectrometric techniques data. Gas chromatography-mass spectrometry. Gas chromatography-infrared spectrometry. Liquid chromatography-mass spectrometry. Section G THERMAL METHODS. Thermogravimetry. Differential thermal analysis and differential scanning calorimetry. Thermomechanical analysis. Evolved gas analysis. Section H SENSORS, AUTOMATION AND COMPUTING. Chemical sensors and biosensors. Automated procedures. Computer control and data collection. Data enhancement and databases. Further reading.
Summary: This title provides concise yet comprehensive coverage of analytical chemistry at an undergraduate level, providing easy access to the core information in the field. It covers all the important areas of analytical chemistry.
Holdings
Item type Current library Call number Copy number Status Date due Barcode
Long Loan TUS: Midlands, Main Library Athlone General Lending 543 KEA (Browse shelf(Opens below)) 1 Available 00212571
Short Loan TUS: Midlands, Main Library Athlone General Lending 543 KEA (Browse shelf(Opens below)) 1 Available 00212570
Short Loan TUS: Midlands, Main Library Athlone General Lending 543 KEA (Browse shelf(Opens below)) 1 Available 128099

Includes bibliographical references (p. 337-338) and index.

Section A NATURE AND SCOPE OF ANALYTICAL CHEMISTRY. Analytical chemistry, its functions and applications. Analytical problems and procedures. Analytical techniques and methods. Sampling and sample handling. Calibration and standards. Quality in analytical laboratories. Section B ASSESMENT OF DATA. Errors in analytical measurements. Assessment of accuracy and precision. Significance testing. Calibration and linear regression. Quality control and chemometrics. Section C ANALYTICAL REACTIONS IN SOLUTION. Solution equilibria. Electrochemical reactions. Potentiometry. pH and its control. Titrimetry I: acid-base titrations. Complexation, solubility and redox equilibria. Titrimetry II: complexation, precipitation and redox titrations. Gravimetry. Voltammetry and amperometry. Conductimetry. Section D SEPARATION TECHNIQUES. Solvent and solid phase extraction. Principles of chromatography. Thin-layer chromatography. Gas chromatography: principles and instrumentation. Gas chromatography: procedures and applications. High-performance liquid chromatography: principles and instrumentation. High performance liquid chromatography: modes, procedures and applications. Electrophoresis and electrochromatography: principles and instrumentation. Electrophoresis and electrochromatography: modes, procedures and applications. Section E SPECTROMETRIC TECHNIQUES. Electromagnetic radiation and energy levels. Atomic and molecular spectrometry. Spectrometric instrumentation. Flame atomic emission spectrometry. Inductively coupled plasma spectrometry. X-ray emission spectrometry. Atomic absorbance and fluorescence spectrometry. Ultraviolet and visible molecular spectrometry: principles and instrumentation. Ultraviolet and visible molecular spectrometry: applications. Infrared and raman spectrometry: principles and instrumentation. Infrared and raman spectrometry: sample preparation and spectral interpretation. Nuclear magnetic resonance spectrometry: principles and instrumentation. Nuclear magnetic resonance spectrometry: interpretation of proton and carbon-13 spectra. Mass spectrometry. Section F COMBINED TECHNIQUES. Advantages of combined techniques. Sample identification using multiple spectrometric techniques data. Gas chromatography-mass spectrometry. Gas chromatography-infrared spectrometry. Liquid chromatography-mass spectrometry. Section G THERMAL METHODS. Thermogravimetry. Differential thermal analysis and differential scanning calorimetry. Thermomechanical analysis. Evolved gas analysis. Section H SENSORS, AUTOMATION AND COMPUTING. Chemical sensors and biosensors. Automated procedures. Computer control and data collection. Data enhancement and databases. Further reading.

This title provides concise yet comprehensive coverage of analytical chemistry at an undergraduate level, providing easy access to the core information in the field. It covers all the important areas of analytical chemistry.

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